Reflection high-energy electron diffraction:
Reflection high-energy electron diffraction (RHEED) is another type of diffraction technique used to characterize the surface of crystalline materials.
• RHEED systems gather information only from the surface layer of the sample and hence quite useful to monitor the growth condition of the materials at different stages:
☆ Substrate thermal cleaning monitoring
☆ Controlling initial growth stage
☆ Monitoring surface structure and growth dynamics
☆ Growth rate measurement
• The small incident angle makes it sensitive to the structure of top monolayers.
RHEED: Principle of operation:
• RHEED is typically based on the reflection of electrons with high kinetic energy (~ 5 - 100 keV) and low impact angle (< 5°) from the surface of a solid.