Module 1 : Introduction

Lecture 2 : Orientation

 

 

 

Process Technology Functional Role

Separators:

    a) Batch distillation
    b) Continuous distillation
    c) Absorption
    d) Stripping
    e) Liquid-liquid extraction
    f) Leaching
    g) Crystallization
    h) Drying
    i) Flash separator
    j) Membrane separator
    k) Packed bed contactor

 


- Most important process technology
- Provides desired separation between phases and streams
- Located next to the reactor as 100 % conversions are very rare in industrial practice

a) Batch distillation column



- Used to separate a liquid mixture based on relative volatility (differences in boiling points)
- Operated in batch mode

b) Continuous distillation (Fractionator)

- The most important separation technology in process flow sheets

- Provides very pure products

- Differences in boiling points is the working principle

- Energy intensive operation

- Usually multi-component distillation is apparent in industrial practice

c) Absorption column

- Used to absorb components from gaseous stream
- Solvent is used
- Usually followed with stripper to re-generate the fresh solvent
- Operated at low temperature and moderate/high pressure

d) Stripper

 


- Steam/Hot gas is used to strip the gas
- Regenerated solvent used for absorption

e) Liquid Liquid extraction



- Used to separate components from a liquid with a liquid solvent
- Consists of a series of mixers and separators
- Produces extract (rich with solvent and components extracted) and raffinate (product with lean extractants)

f) Leaching

 

- A liquid solvent extracts components from a solid
- High interfacial area between solid/liquid is required to enhance extraction capability

g) Crystallization

- Used to crystallize solids from a slurry/super-saturated solution

- Fine crystals added to serve as nucleating agent

h) Spray drier

 



- Liquid slurry is sprayed in the form of droplets

- Hot gas (air) dries the solid

- Enables very good control over the product particle size

i) Rotary drier

 

- Through rotation, an agitated liquid film is dried to obtain the dried solid.

j) Flash separator

 

- Very common technology to separate liquid streams at high pressure and lower temperatures.

- Upon pressure reduction/heating, low boiling components separate as vapor phase and yield a liquid phase.

- Complete separation only possible for fewer components
k) Membrane separation
- A semi-permeable barrier (membrane) is used to separate feed streams based on concentration difference/pressure difference.

- Various types of processes available

- New technology in process industries.

l) Packed bed contactor

 

- Used for absorption/stripping operations


- Packing serves to enhance gas/liquid interfacial area