Module 7 : Process Design of Mass Transfer Column

Lecture 4 : Hand on Design

 

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From the Figure 7.8: ; Rmin = 0.67 for xD =0.95

Here, reflux ratio , R =2.5 × Rmin =2.5 ×0.67= 1.675 is taken for this design.

Average molecular wt. of feed= 0.5×58 + 0.5×18=38

 

Molar feed flow (F) rate=25,000/38=657.9 kmol/h

Acetone balance: kmol/h

Vapor flow (V) rate above feed plate, 926.2 kmol/h

(Assuming constant molar overflow)

Top section liquid flow rate, L = V - D = 580 kmol/h

Bottom product: B = F - D = 657.9 - 346.2 = 311.7 kmol/h

Mass balance below feed plate:

Slope of the bottom section operating line (Figure 7.8):

= Liquid flow rate below feed plate = 1285.7 kmol/h

= Vapor flow rate below feed plate = 974 kmol/h

 

The construction of operating lines and number of theoretical stages are shown in this Figure 7.8.

Total number of tray= 6 (above feed) +3 (below feed) = 9

Total number of real stages (60% column efficiency; reboiler was considered as equivalent to one theoretical tray)

Figure 7.8: McCabe-Thiele construction.